Nutech 8910ODS Preconcentrator for ODS and Fluorinated Greenhouse Gas Analysis

Nutech 8910ODS Preconcentrator for ODS and Fluorinated Greenhouse Gas Analysis

The Nutech 8910ODS Preconcentrator is a high-performance sample preparation system designed for ultra-trace analysis of ozone depleting substances (ODS) and fluorinated greenhouse gases in ambient air. The system uses inert-treated sample pathways, ultra-clean valves, two-stage cryogenic trapping, and precise temperature control to help minimize contamination, carryover, and analyte loss.

Featuring an industry-leading concentration ratio of over 1000:1 and detection limits down to 0.01 ppbv, the 8910 ODS empowers laboratories to meet the most stringent regulatory requirements for atmospheric monitoring. Its fully automated operation, combined with intuitive Windows-based control software, ensures maximum productivity with minimal operator intervention.

Features of Nutech 8910ODS Preconcentrator

Ultra-trace sensitivity for demanding air analysis

Achieve trace-level detection for ODS and fluorinated greenhouse gas applications with a detection limit down to 0.01 ppbv and a concentration ratio greater than 1000:1. The system is suitable for low-level ambient air monitoring as well as method-driven environmental analysis.

Two-stage cryogenic trapping for enhanced focusing

The 8910ODS combines a HayeSep D adsorbent trap with a cryofocusing trap, both operating across a temperature range of -190°C to 250°C. This two-stage design helps improve analyte enrichment, peak focusing, and chromatographic performance for volatile target compounds.

Inert sample pathway to reduce carryover and contamination

All critical sample pathways are inert-treated, helping reduce surface activity, adsorption, residual contamination, and VOC release from internal components. This supports better sample integrity, higher recovery, and improved reproducibility for trace-level analysis.

High-efficiency water removal without ODS loss

The integrated water removal module uses Nafion-based drying technology, delivering >99% water removal efficiency while avoiding adsorption loss of ODS components. Heated, inert-treated lines further help preserve sample representativeness and reduce interference from water peaks.

Flexible sample volume range

A broad sample introduction range of 4–2000 mL allows laboratories to adapt the method to different sensitivity requirements and sample concentrations. With optional quantitative loop configuration, the minimum injection volume can be extended to 0.1 mL, supporting high-concentration or special-method applications.

Automated operation and productivity upgrade

When paired with the Nutech 3610 autosampler, the system supports up to 16 canister positions for automated sequence operation. Users can set sample sequence, volume, timing, and method parameters to reduce manual intervention and improve laboratory throughput.

Designed for GC and GC/MS integration

The 8910 ODS is designed to integrate with GC, GC/ECD, and GC/MS systems. Remote-control communication enables coordinated GC readiness, start, and wait commands, supporting streamlined operation in routine analytical workflows.

Built-in software control and QA/QC support

The Windows-based control software allows users to edit methods, create sequences, run single or batch tasks, perform system purge, bake traps, flush sample lines, conduct leak checks, and generate QA/QC reports. This supports consistent operation and easier method management.

Nutech ODS & F-GHGs Analysis Solution

Chromatogram of 37 ODS & F-GHGs

Specifications of Nutech 8910ODS Preconcentrator

ParameterSpecification
Detection limit0.01 ppbv
Preconcentration ratio>1000:1
Precision≤3% RSD
Sample volume range4–2000 mL
Optional minimum injection volume0.1 mL
Temperature control accuracy±2°C
Maximum heating rate10000°C/min
Trap 1HayeSep D adsorbent trap, -190°C to 250°C
Trap 2Cryofocusing trap, -190°C to 250°C
Operating environment20–35°C, RH <85%
Maximum power1 kW

Typical Applications

Environmental air monitoring
Trace-level analysis of ODS and fluorinated greenhouse gases in ambient air.

Industrial park monitoring
Monitoring of ozone-depleting substances and hydrofluorocarbons in industrial park environments.

Third-party testing laboratories
Routine canister-based air sample preconcentration and GC/GC-MS analysis.

Research institutions
Low-level atmospheric research, method development, and laboratory studies involving volatile trace compounds.

Regulatory and compliance-driven analysis
Applications requiring standardized sample preconcentration workflows for ODS and fluorinated greenhouse gas monitoring.

Background: ODS and Fluorinated Greenhouse Gases

Ozone-depleting substances (ODS) are a group of halogenated chemicals that can damage the Earth’s stratospheric ozone layer. Historically, they have been widely used as refrigerants, cleaning agents, foam-blowing agents, and fire-extinguishing agents. Major ODS categories include chlorofluorocarbons (CFCs), halons, carbon tetrachloride (CTC), methyl chloroform (1,1,1-trichloroethane), hydrochlorofluorocarbons (HCFCs), hydrobromofluorocarbons (HBFCs), bromochloromethane (BCM), and methyl bromide.

Once released into the atmosphere, these compounds can persist for long periods and eventually reach the stratosphere. Under ultraviolet radiation, they release chlorine or bromine radicals, which catalytically destroy ozone molecules. The resulting depletion of the ozone layer allows increased levels of ultraviolet radiation to reach the Earth’s surface, posing risks to human health, ecosystems, agriculture, and the broader biosphere.

Hydrofluorocarbons (HFCs), while not ozone-depleting, were introduced as substitutes for many phased-out ODS. However, many HFCs have high global warming potentials and are now subject to increasing regulatory control due to their contribution to climate change.

FAQ of Nutech 8910ODS Preconcentrator

The Nutech 8910ODS Preconcentrator is used for the preconcentration and thermal desorption of volatile compounds in gas samples. It is typically coupled with GC/MS systems for the quantitative analysis of ozone-depleting substances and fluorinated greenhouse gases in ambient air and related gas samples.

The system is designed for gas samples collected in inert-treated evacuated canisters. After preconcentration and thermal desorption, the analytes are transferred to the GC or GC/MS system for chromatographic separation and detection.

The instrument includes preset application methods and is intended to support manual monitoring methods for ozone-depleting substances and fluorinated greenhouse gases, including applications related to ambient air and industrial park monitoring.

The detection limit is 0.01 ppbv. Actual method detection limits may vary depending on the GC/MS configuration, target compound list, injection volume, analytical method, background contamination, and laboratory conditions.

The preconcentration ratio is specified as greater than 1000:1, enabling trace-level analysis by enriching a relatively large gas sample volume before chromatographic analysis.

The specified precision is ≤3% RSD under the conditions defined by the instrument method and operating procedures.

The standard sample introduction range is 4–2000 mL. With an optional quantitative loop, the minimum injection volume can be extended to 0.1 mL, allowing the system to handle samples across different concentration ranges.

The 8910 ODS uses two cryogenic stages: a HayeSep D adsorbent trap and a cryofocusing trap. Both traps operate from -190°C to 250°C. This configuration supports analyte enrichment, moisture management, thermal desorption, and peak focusing before GC or GC/MS analysis.

Liquid nitrogen is used to cool the traps to cryogenic temperatures, with the lowest trap temperature reaching approximately -190°C. This is necessary for efficient trapping and focusing of volatile analytes. Proper handling is required to prevent frostbite and ensure safe operation.

The water removal module is a required component. Without it, water-containing calibration gases or samples may produce significant water peaks that interfere with target compound peak shape and analytical performance.

The module uses Nafion-based drying and is specified to achieve over 99% water removal efficiency. The manual notes that this drying approach avoids adsorption loss of ODS components and helps meet the high water-removal requirements of ODS analysis.

The instrument uses inert-treated tubing and ultra-clean valves to reduce adsorption, carryover, contamination, and VOC release from internal surfaces. This is especially important for trace-level analysis, where even small background contributions may affect blanks and quantitation.

The system typically requires high-purity helium as carrier gas and sweep gas, nitrogen or compressed air for heating gas, dry nitrogen for the water removal module, liquid nitrogen for cryogenic cooling, and appropriate calibration gases depending on the analytical method.

The system typically requires high-purity helium as carrier gas and sweep gas, nitrogen or compressed air for heating gas, dry nitrogen for the water removal module, liquid nitrogen for cryogenic cooling, and appropriate calibration gases depending on the analytical method.

Yes. If no autosampler is installed, a terminal plug must be installed at the autosampler interface; otherwise, the preconcentrator may report an error. In this configuration, sample introduction should use the appropriate sample inlet on the main unit.

The optional 3610 autosampler provides automated sample introduction, with 16 sample positions and compatibility with different canister sizes, including 1/3/6/15 L canisters. It supports programmed sample sequences, volumes, and timing parameters, reducing manual intervention.

Yes. The manual states that the autosampler uses inert-treated internal lines and supports functions such as automatic leak checking, heating, and backflushing. These are intended to reduce sample contamination and carryover.

The Windows-based control software supports method editing, sequence creation, sequence operation, system purge, trap bakeout, sample line flushing, leak checking, manual control, QA/QC reporting, and system error information. The real-time interface displays temperature zones, valve actions, gas flow direction, and operating status.

Before running a sequence, operators should confirm that the instrument is connected, the system has passed self-check, parameters have not been lost, the instrument has reached the ready state, and the selected sequence contains the correct sample type, inlet position, sample volume, and method file.

Possible causes include insufficient gas purity, contaminated carrier gas, leaks in the preconcentrator or GC/MS transfer line, ineffective hydrocarbon or moisture traps, improper laboratory environment, residual contamination in sample pathways, or use of non-original consumables. The manual recommends high-purity gases, hydrocarbon traps where needed, leak checking, and GC/MS air/water checks after leak testing.

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