Why is my measurement response low at high concentrations?
Most likely cause: Leakage in sampling line or internal tubing This dilutes the sample and leads to underestimation.
Most likely cause: Leakage in sampling line or internal tubing This dilutes the sample and leads to underestimation.
Possible causes include: Incorrect H₂ or air flow rates Leaks in the system Blocked FID nozzle Faulty ignition wire or voltage output In real use, 80% of ignition failures are flow or leak related—not hardware failure.
Before shutdown: Purge with clean ambient air for 3–5 minutes Ensure no high-concentration residue remains Otherwise: VOCs may condense in tubing This leads to memory effects and false readings
Because: FID response is affected by oxygen concentration Water vapor dilutes hydrocarbon concentration These corrections ensure results are: Comparable Closer to regulatory reporting basis (dry gas, corrected values)
Use a standard gas close to sample concentration (≈80% of span) Inject via sampling line or span port Select a stable reading and input standard concentration
Zero calibration ensures the baseline of the FID is accurate. Perform after stabilization Takes about 30 seconds Can be done via “Zero Calibration” or Auto Zero function
Before startup, you should: Ensure all tubing and cables are properly connected Check filters on the sampling line Confirm H₂ cartridge is installed and connected Make sure power supply meets requirements
The instrument typically requires at least 15–20 minutes of preheating after ignition to stabilize before performing zero calibration or measurements.